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Geo-spatial location, chronological period, research sample (gender, age, etc. Farmakope Indonesia edisi IV, Jakarta: Departemen Kesehatan Republik. PHARMACY: Jurnal Farmasi Indonesia (Pharmaceutical Journal of Indonesia) Jurnal Pharmacy, Vol. Pharmacy Faculty, Universitas Muhammadiyah Purwokerto /rebates/&252fdownload-farmakope-indonesia-edisi-4-tahun-1995-pdf.
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Keywords: chloramphenicol, reversed phase HPLC, eye drop. Microsoft Windows / Portable Document Format / Operating System Families / Computing Platforms / Ibm Pc Compatibles. The sample was fulfilled the requirement of Farmakope Indonesia fourth edition. Sesuai dengan amanat Undang-Undang No 36 Tahun 2009 tentang Kesehatan Pasal 105 Sediaan Farmasi yang berupa obat dan bahan baku obat harus memenuhi syarat Farmakope Indonesia atau buku standar lainnya, Farmakope memegang peranan penting dalam jaminan mutu obat pada saat proses.
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The average chloramphenicol content of generic and branded product were 117.6 and 111.29% respectively. Download Gratis Farmakope Indonesia edisi V Filetype PDF. The precision test showed coefficient variation (CV) was 5.988%. The equation of regression was y=1.6429x – 5.5758 with LOD and LOQ were 5.2 and 17.3 µg/mL respectively. Determination of calibration curve linearity showed linear correlation between the peak area and concentration at 10-30 µg/mL with correlation coefficient r=0.990. The Shimpack ODS CLC C18 column was used as stationary phase, methanol:water (40:60) v/v as mobile phase, with flow rate 1 mL/minute. Kata kunci: kloramfenikol, KCKT, tetes mataĭetermination of Chloramphenicol in generic and branded eye drop had been carried out by reversed phase high performance liquid chromatography (HPLC) method with UV detector (280 nm). Berdasarkan pengujian, sampel tetes mata generik dan bermerek memenuhi persyaratan yang tertera pada Farmakope Indonesia edisi IV. Hasil penetapan kadar kloramfenikol dalam tetes mata pada sediaan generik adalah 117,6% dan dalam tetes mata bermerek sebesar 111,29%. Uji presisi memberikan hasil nilai koefisien variasi sebesar 5,988%. Nilai limit of detection (LOD) sebesar 5,2 µg/mL dan nilai limit of quantitation (LOQ) sebesar 17,3 µg/mL. Persamaan regresi yang diperoleh adalah y=1,6429x- 5,5758. Penentuan linearitas dengan kurva baku menunjukkan hubungan yang linier antara luas puncak dan konsentrasi baku kloramfenikol dengan konsentrasi 10-30 µg/mL (r=0,990). Fase diam yang digunakan adalah kolom Shimpack ODS CLC C18, fase gerak metanol:air (40:60) dengan kecepatan alir 1 mL/menit. Telah dilakukan penetapan kadar kloramfenikol dalam tetes mata pada sediaan generik dan merk menggunakan Kromatografi Cair Kinerja Tinggi (KCKT) fase terbalik dengan detektor ultraviolet pada panjang gelombang 280 nm. 24 (2001) 755–767.PENETAPAN KADAR KLORAMFENIKOL DALAM TETES MATA PADA SEDIAAN GENERIK DAN MERK DENGAN METODE KROMATOGRAFI CAIR KINERJA TINGGI Brittain (ed.) Profile of Drug Substances, Excipients and Related Methodology, Vol. Donnervert, Qualitaetssicherung in der Analytischen Chemie, VCH Weinheim, New York-Basel-Cambrige, 1992, pp.
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ISO (Informasi Spesialite Obat) Indonesia, Volume XXXVII, Ikatan Sarjana Farmasi Indonesia, Jakarta, 2008.įarmakope Indonesia, edisi IV (Indonesian Pharmacopoei IV), Departemen Kesehatan Republik Indonesia, Jakarta, 1995.Ĭ.S.P.
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CD-ROM Version, Pharmaceutical Press, The Royal Pharmaceutical Society of Great Britain (PhP), London, 2007. Buku farmakope indonesia edisi 4.pdf - ebook and manual Free pdf ebooks (users guide, manuals, sheets). Sweetman (ed.), Martindale 35: The Complete Drug Reference. The peak of mebhydrolin napadisylate was not interfered by those of possible degradation products. The drug was subjected to acidic and alkaline hydrolysis, oxidation, dry heat, and UV treatment. The detection limit and quantification limit were 18.5 and 55.5 ng/spot, respectively.
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The RSD of repeatability and intermediate precision were found to be less than 2%, whereas the mean of the recovery data was 99.3–100.8%. Good linearity was achieved in the concentration range 600–1600 ng/spot. The method was validated for specificity, linearity, accuracy, precision, and robustness. Quantitative evaluation was performed by measuring the absorbance reflectance of the analyte spots at 287 nm. After extraction of the analyte with a mixture of methanol and NH 4 OH 25% (100:1.5, v/v), the extracts were spotted on precoated HPTLC silica gel F254 plates, which were developed with a mixture of methanol and ethyl acetate (1:1, v/v). A simple and rapid high-performance thin-layer chromatography (HPTLC) densitometric method has been developed for the determination of mebhydrolin napadisylate in tablets.